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1 article(s) from Krentsel, Liya B

Cross-metathesis of polynorbornene with polyoctenamer: a kinetic study

Yulia I. Denisova,
Maria L. Gringolts,
Alexander S. Peregudov,
Liya B. Krentsel,
Ekaterina A. Litmanovich,
Arkadiy D. Litmanovich,
Eugene Sh. Finkelshtein and
Yaroslav V. Kudryavtsev

Beilstein J. Org. Chem. 2015, 11, 1796–1808, doi:10.3762/bjoc.11.195

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Graphical Abstract

Figure 1: Dependences of the (blue) PCOE and (green) PNB mean hydrodynamic radius [Graphic 2] in CHCl₃ on the (a) light ...

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Figure 2: Hydrodynamic radius distributions (normalized by their maximum values) in the CHCl₃ solutions of (b...

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Figure 3: Stability of the primary carbene [Ru]=CHPh in the pure solvent (CDCl₃).

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Scheme 1: Formation of polyoctenamer-bound carbene by the interaction of Gr-1 with PCOE.

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Figure 4: (a) Dependences of the normalized (red) [Ru]=CHPh and (blue) [Ru]=PCOE carbene concentrations on ti...

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Scheme 2: Formation of polynorbornene-bound carbene by the interaction of Gr-1 with PNB.

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Figure 5: (a) Dependences of the normalized (red) [Ru]=CHPh and (green) [Ru]=PNB carbene concentrations on ti...

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Scheme 3: Elementary cross-metathesis reactions in the mixture of PCOE with PNB.

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Figure 6: Dependences of the normalized (red) primary, (blue) PCOE, and (green) PNB carbene concentrations an...

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Figure 7: The kinetics of NB-COE dyads formation under mixing conditions for the systems with (red) c_in/c_p = ...

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Figure 8: The ¹H NMR spectrum recorded after 10 min of the reaction between PCOE and Gr-1 at the initial conc...

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Figure 9: The ¹H NMR spectrum recorded after 653 min of the reaction between PNB and Gr-1 at the initial conc...

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Figure 10: The ¹H NMR spectrum recorded after 24 h of the reaction between PCOE, PNB, and Gr-1 at the initial ...

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Figure 11: The ¹³C NMR spectrum recorded after 8 h of the reaction between PCOE, PNB, and Gr-1 at the initial ...

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Published 01 Oct 2015

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